• To introduce participants to advanced gas chromatography and how the individual elements interrelate.
• To be able to competently use and develop methods on a gas chromatograph to produce robust and valid analytical data.
• To provide advanced knowledge of gas chromatography operation, maintenance and troubleshooting.
• To impart the participants advance techniques and knowledge of gas chromatography.
• To provide knowledge of accessories and consumables required for gas chromatography operations.
• To provide good laboratory practices for accurate and reliable analyses.
• To train participants to know how to change and install gas chromatography parts such as inject systems and columns.
• To familiarize participants with the techniques used in gas chromatography analysis, qualitative and quantitative methods.

The course is designed for chemists, lab technicians, chemical engineers, instrument engineers and lab supervisors/managers.

This interactive Training will be highly interactive, with opportunities to advance your opinions and ideas and will include;

• Lectures
• Workshop & Work Presentation
• Case Studies and Practical Exercise
• Videos and General Discussions

Module One:

• Introduction
• History of Chromatography
• Type of Chemical Analysis
• Separation Analysis
o Separations in everyday life
o Simple separation procedures
o Classification of separation process
o Chromatographic Separation
o Types of Separation Chromatography
• Symbols and terms of Chromatography
• Physical forces and interactions chromatography
• Fundamentals of chromatography
o Definitions
o Basic System Design
o Concept of Polarity
o Properties of Separation
o Physiochemical Processes of Separation
o Adsorption
o Partition
o Ion Exchange
o Size Exclusion

Module Two:

• Type of Chromatographic Analysis
• Gas Chromatography
• Objectives & Definitions
• Principals of GC
• Mobile and Stationary Phase
• Instrumentation of Gas Chromatography

• Mobile Phase
• Gas Supplies
• Sample Introduction, Injection Ports and Valves
o Packed Column Injectors
o Open Tubular Column Injectors
o Injection Methods and Techniques
o The role of sample introduction and injection ports in GC operations
o Injection ports maintenance and its impact on GC performance

Module Three:

• Columns
o Open Tubular Capillary GC Column
o Packed GC Column
o Configurations of the stationary phase
o Column selection & maintenance
o Selecting Stationary Phases
o How columns can impact GC performance

• Detectors
o Flame ionization Detector
o Thermal Conductivity Detector
o Other Detectors
o Detector Selection
o The role of Detectors in GC operations
o Detector maintenance
o How detectors can impact GC performance
• GC operation
o Setup and GC Operation, Basic steps
o Sampling Techniques
o Programmed Temperature GC
o Peak Dispersion in a Chromatographic Column
o Your First Chromatogram
o From Chromatograms to Report

Module Four:

• Maintenance and troubleshooting
o Errors in Qualitative and Quantitative Analysis
o Correction of errors and improving accuracy
o Preventive maintenance
o Routine Maintenance
o Practical application for schedule maintenance
o How to replace spare parts
o Troubleshooting fixation
• Evaluation of GC
• Data Acquisition and Calibration
o Recorders & Data Acquisition
o Data analysis
o Data Acquisition and Processing
o Data Processing
o Calibration
o Data Acquisition and Processing System
o Calibration linked to GC performance
• Data Results
o Recorders & Data Acquisition
o Data analysis
o Data Acquisition and Processing
o Data Processing

Module Five:

• Application in analysis by Gas Chromatography
o Analysis of Non-volatiles
o Water sample & Inorganic GC
o Organic and petroleum samples
o Qualitative & Quantitation Analysis Strategies
o Performing Trace Analysis
o Errors in Qualitative and Quantitative Analysis
o Chemical laboratory measurement evolution
• Method Development & validation
• Quality Control & Quality Assurance
o Statistical in analytical methods
o Data Validation of analysis results
o Quality Assurance Program
o Evaluation of analytical data
o Study Performance and Reporting

BTS attendance certificate will be issued to all attendees completing minimum of 80% of the total course duration

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