By the end of this course delegates will be able to:

• To impart participants fundamental techniques of analytical chemistry.
• To identify the application of analytical methods.
• To understand the instruments’ techniques.
• To know how to judge the accuracy and precision of experimental data and how these judgments can be sharpened by the application of statistical methods.
• To understand the tools and techniques used to achieve process analysis, qualitative methods, cause and effect diagrams and calibration graphs.
• To be familiar with the latest analytical methods.

The course is designed for chemists, lab technicians, chemical engineers, instrument engineers and lab supervisors/managers.

This interactive Training will be highly interactive, with opportunities to advance your opinions and ideas and will include;

• Lectures
• Workshop & Work Presentation
• Case Studies and Practical Exercise
• Videos and General Discussions

Module One:

• Introduction
• Historical and review
• Analytical Chemistry and Chemical Analysis
• Type of Chemical Analysis Methods
o Classical Methods
o Instrumental Methods
• Instrumental analysis in laboratory
• Basic Principle and theory of Instrumental Analysis
• Rules for operation laboratory instruments
• Spectroscopic Instrumental Analysis
o Molecular Spectroscopy analysis
 UV-Vis spectroscopy
 FTIR Spectroscopy

Module Two:

o Atomic Spectroscopy analysis
 X-ray analysis (XRF-XRD)
 Atomic Absorption Spectrometry (AAS)
 Atomic Emission Spectrometry (AES)
 Inductively Coupled Plasma (ICP)
• Separation Instrument Analysis
o Gas Chromatography
o High Performance Liquid Chromatography
o Ion Chromatography
• Electrochemical Instrument analysis
o pH meter
o Conductivity meter
o DO meter
o KF water analysis

Module Three:

• Computerized Systems, Good Automated Laboratory Practices
• Choosing the Right Instrument
• Comparing Instrumental Techniques
• Comparing Online Analyzers and Laboratory Instruments
• How to prepare tender for new instrument and consumable
• FAT Factory Acceptance Test & SAT Site Acceptance Test
• Chemical laboratory measurement evolution
o Reporting results
o Significant Figure Rules
o Laboratory Certification
o The Evaluation of Results and Methods

Module Four:

• Instrumentals Calibration, and Standardization
o History of Calibration Requirements
o Instruments Calibration and Traceability
o Standard Reference Materials
o Methodologies for a Calibration Program
 Standard calibration
 Internal Standard calibration
 External Standard calibration
 Correction of errors and improving blank
 Correlation Coefficient & Residual analysis in regression
 Quality / Calibration Manual
 Calibration work instructions, procedures, certificate, and documentation
 Calibration Reports, and Records Requirements

Module Five:

• Measurement Uncertainly in testing and calibration
• Type of errors in instrumental analysis
o Systematic, Random, and Gross errors
o Correction of errors and improving accuracy
o Precision Equipment Handling

• Maintenance and troubleshooting in instrumental analysis
o Routine & Preventive Maintenance
o Troubleshooting, Corrective and Preventive Action
• How to used LIMS in improvement laboratory instrument
• Establishing the traceability of measurements
• Measurement Uncertainly in testing and calibration
• Estimation of Measurement Uncertainty
o Standard Uncertainty
o Expanded Uncertainty

BTS attendance certificate will be issued to all attendees completing minimum of 80% of the total course duration.

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